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Isopropyl Extraction Attempt: Gooey Gooey Goodness

kl.metacog

Kava Enthusiast
I was debating back and forth about doing an acetone extraction but decided against it because a) my roommates wouldn't appreciate the whole house smelling like nail polish remover b) I can't obtain the quality of acetone that I would feel comfortable with.  An Isopropyl extraction however made it easy to obtain a solvent without impurities (alcohol + water) and it was cheap to boot!  However, it did make the whole first floor smelling like rubbing alcohol, even with all the windows open and a fan going.  CAUTION: SOLVENTS LIKE ALCOHOL/ACETONE ARE EXTREMELY FLAMMABLE AND THE FUMES CONSIDERED HARMFUL.  KEEP YOUR WORK AREA OUTSIDE OR VERY, VERY WELL VENTILATED AND DISCOURAGE THE PRESENCE OF AN OPEN FLAME.
Also, I obtained the steps for the process from various cannabis/drug forums so the process is not my own in any way.

The usual culprits plus some newbies:

The first step was to combine the alcohol and root in the jar.  I used a half cup root and poured in the Iso until the powder was submerged.  I then furiously shook the thing for 2 minutes as suggested by the interwebs.  This was then filtered using an ultra high tech filtering system (toilet paper and a funnel) into a lab-grade container (beer glass).



The result of which ten minutes later. . .


Now the fun part:  As you can see the system is pretty simple.  There's a saucepan on the bottom full of water, with a plate containing the solution on the top.  The temperature of the steam heats the alcohol to a sufficient temperature to induce evaporation. I DON'T RECOMMEND THIS METHOD IF YOU HAVE A GAS STOVE.  I used medium-high heat since full-high was too scary.  As I stated earlier, the smell permeated the kitchen quite intensely.  There's no way you can get away with doing this without the whole house knowing, unless maybe you have a bad ass hood over your stove.
Oh and sorry our kitchen is gross.  We're college students.

About 7-10 minutes in:



20 minutes in.  The lighter highlights of the dark spot are bubbles.  Once these disappeared and there didn't seem to be any liquid left I pulled off the plate and allowed it to cool.  I moved the plate around and upside down, but there wasn't any type of flow happening (which would've indicated there was still iso left)  just gooey, gooey goodness.

Got out a razor blade and went to work.  Verrrry sticky!  Which is where I ran into an important problem:  How to transfer it?!  I really couldn't think of anything really but wax paper, so that's what I did.  Definitely lost about 10-15% in the process trying to get this shit from the plate to the razor blade to the paper.  If anybody has any ideas let me know!


Once I got it on the paper I threw it in the freezer so it'll be easier to work with.  Should take a couple hours or so.


I might sample some tonight or tomorrow, not sure yet.  I'll be sure to post the results.
 

krunkedout

Kava Lover
Looks pretty good! If you want to get the rest off the plate the. Just poor a small amount of the iso on the plate and then poor that on the wax paper and let it evap there
 

kl.metacog

Kava Enthusiast
Yeah that could work.


Well, in case anyone was wondering smoking it is a bust. My friends and I were bored and decided to make a parsley/resin joint with it. Tasted like shit and the effects were very mild at best.


However, a little dab sublingually seems to be doing the trick. Definitely a formidable buzz beyond placebo. However, like the oil extract it seems to be more head-focused.
 

kavadude

❦ॐ tanuki tamer
Alcohol extracts have a higher concentration of the hepatotoxic (liver toxic) compound flavokawain B. Don't wanna discourage science but be careful.
 

kl.ImSoCold2323

Kava Curious
What?! Proof to back up random claims about kava?  Preposterous!  I've been asking for that for years...
Actually, I think I remember an old thread about this.  I'll see if I can find it.
 
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